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- W2382981812 abstract "1-[2-(N,N-Dimethyl-amino)ethyl]-1H-tetrazol-5-thiol was prepared from N,N- dimethylaminoethyldiamine by addition reaction,esterification and via 1,3-dipolar cycloaddition with sodium azide finally.The optimal reaction conditions were as follows: n(N,N-dimethylaminoethyldiamine):n(carbon bisulfide):n(dimethyl sulfate):n(sodium azide)=1:1:1.3:0.94,the addition temperature was 10℃～15℃;the esterification temperature was 10℃～15℃,the reaction lasted 3h;the cycloaddition was carried out under temperature of 65℃for 6h and the total yield was 69.2%." @default.
- W2382981812 created "2016-06-24" @default.
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- W2382981812 date "2008-01-01" @default.
- W2382981812 modified "2023-09-23" @default.
- W2382981812 title "Preparation of 1-[2-(N,N-Dimethyi-amino)ethyl]-1H-tetrazol-5-thiol" @default.
- W2382981812 hasPublicationYear "2008" @default.
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