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- W2383103663 abstract "2-(2′-hydroxy-5′-methylphenyl)benzotriazole-N-oxide was synthesized from azo-compound with hydrazine hydrate as a reducing agent.The effect of the molar ratio of reactants,the amount and concentration of sodium hydroxide on the product was studied.Experimental results showed that,the best molar ratio of azo-compound,hydrazine hydrate and sodium hydroxide is 1∶0.53∶5.3,the concentration of sodium hydroxide was 18%,and the reaction temperathre was from 80 to 82℃,under above conditions the reaction yield could be higher than 95% with the purity of products up to 99%." @default.
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- W2383103663 date "2007-01-01" @default.
- W2383103663 modified "2023-09-26" @default.
- W2383103663 title "Synthesis of 2-(2′-hydroxy-5′-methylphenyl)benzotriazole-N-oxide" @default.
- W2383103663 hasPublicationYear "2007" @default.
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