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- W2383208840 abstract "OBJECTIVE:To establish gas chromatography(GC)for simultaneous determination of the contents of 9 organochlorine pesticides in licorice root medicinal material.METHODS:The determination of contents was performed by GC,briefly,capillary column DB-1701(30 m×0.25 mm,0.25 μm)was used,with injection port temperature kept at 220 ℃;column temperature kept at 140 ℃ for 1 min then raised to 210 ℃ at an increasing rate of 10 ℃/min,with the temperature retained for 1 min then raised to 260 ℃ at an increasing rate of 20 ℃/min,with this temperature retained for 20 min;the detector temperature was kept at 300 ℃;the carrier gas was high purity nitrogen(99.999%)at a flow rate of 1.0 ml/min in constant current mode without split flow with injection volume of 1 μl.RESULTS:The linear ranges of the 9 organochlorine pesticides were 1-250 ng/ml.The average recovery rate was 102.40% with RSD of 2.12%(n=9).CONCLUSION:The GC method is simple,rapid and accurate,and it is suitable for the content determination of 9 organochlorine pesticides in licorice root medicinal material." @default.
- W2383208840 created "2016-06-24" @default.
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- W2383208840 date "2013-01-01" @default.
- W2383208840 modified "2023-09-23" @default.
- W2383208840 title "Determination of 9 Organochlorine Pesticides in Licorice Root Medicinal Material by Gas Chromatography" @default.
- W2383208840 hasPublicationYear "2013" @default.
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