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- W2383239563 abstract "A flow injection-chemiluminescence(FI-CL) method based on molecular imprinting-solid phase extraction has been developed for the determination of maleic hydrazide(MH) in vegetables.This method was based on the enhancement effect of MH on chemiluminescence intensity of galangin-potassium permanganate-polyphosphoric acid system.A molecular imprinting polymer(MIP) was synthesized from the thermally initiated polymerization of MH as a template molecule,methacrylic acid as a functional monomer and ethylene glycol dimethacrylate(EGDMA) as a cross-linker and azodiisobutyronitrile(AIBN) as an initiator and used to prepare a solid phase extraction column.Samples were subjected to solid phase extraction before CL assay.Under optimized conditions,relative CL intensity showed good linear relationship with MH concentration in the range from 5.0 × 10-5to 3.0 × 10-2mg/mL.The limit of detection of this method was 2.6 × 10-5mg/mL(3σ).The precision(RSD) for 10 replicate determinations of a known concentration of MH(1.0 × 10-3mg/mL) was 2.7%.In the determination of potato,onion and garlic by this method,average spike recovers of MH were in the range from 95.2% to 111.7% with RSD 1.8% for potato,2.4% for onion and 2.1% for garlic,respectively." @default.
- W2383239563 created "2016-06-24" @default.
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- W2383239563 date "2012-01-01" @default.
- W2383239563 modified "2023-09-22" @default.
- W2383239563 title "Determination of Maleic Hydrazide in Vegetables by Molecularly Imprinting Solid Phase Extraction-Chemiluminescence Method" @default.
- W2383239563 hasPublicationYear "2012" @default.
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