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- W2383601810 abstract "A method was developed for the determination of 19 acidic pesticides in fruit by dispersive solid phase extraction and liquid chromatography-tandem mass spectrometry(LC-MS/MS).The 19 analytes were extracted from the fruit samples by acetic acid-acetonitrile(1 ∶ 99,V/V),and purified by dispersion solid phase extraction using C18 sorbent,and then analyzed by liquid chromatography-tandem mass spectrometry(LC-MS/MS).The 19 analytes were then separated on a reversed phase column using a gradient elution program of aqueous solution containing 0.1% formic acid aqueous solution and 0.1% formic acid acetonitrile solution.Qualitative analysis was performed using multiple-reaction monitoring(MRM).Matrix-matched calibrations were respectively used to quantify the residue concentrations.The recoveries were in the range of 70.3%-105.3%,and the relative standard deviation(RSDs) were 0.4-10.9% at 0.02 mg/kg,0.05 mg/kg and 0.1 mg/kg three spiked levels for all analytes.The limits of quantification(LOQ) for all analytes were between 0.005 mg/kg and 0.02 mg/kg." @default.
- W2383601810 created "2016-06-24" @default.
- W2383601810 creator A5037529581 @default.
- W2383601810 date "2013-01-01" @default.
- W2383601810 modified "2023-09-23" @default.
- W2383601810 title "Determination of 19 Acidic Pesticide Residues in Fruit by Dispersive Solid Phase Extraction and Liquid Chromatography-Tandem Mass Spectrometry" @default.
- W2383601810 hasPublicationYear "2013" @default.
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