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- W2383972012 abstract "Objective:To establish a liquid chromatography-tandem mass spectrometry(LC/MS/MS)method for determining the concentration of rocuronium in plasma.Methods:After addition of vecuronium as internal standard(IS),plasma samples were precipitated by acetonitrile.The separation was carried out on an Atlantis Hilic Silica column(50mm×2.1mm,5μm) with a mobile phase of acetonitrile-ammonium acetate(20mmol·L-1,pH 3.0)(78∶22) at a flow rate of 300μL·min-1.Samples were detected in positive mode with a Turboion Spray source.Results:A good linearity was obtained in the range of 0.02~4mg·L-1(r=0.9992).The RSDs of inter-batch and intra-batch were both less than 12%.All the samples were stable after three freeze thaw cycles.Conclusion:It is an accurate,sensitive and rapid method that can be applied to the validation of Target-Controlled Infusion(TCI) of rocuronium in whole anesthetized patient plasma,which can lead to a reliable result." @default.
- W2383972012 created "2016-06-24" @default.
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- W2383972012 date "2008-01-01" @default.
- W2383972012 modified "2023-09-23" @default.
- W2383972012 title "Determination of plasma rocuronium by liquid chromatography-tandem mass spectrometry and its clinical application" @default.
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