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- W2384037426 abstract "An HPLC method was developed for the quantitative determination of cefquinome sulphate residues in swine tissues.The HPLC system consisted of C18 column(4.6 mm ×150 mm,5 μm) and the mobile phase was 3.45 g perchlorate in 1 000 mL water-phosphates 12 mL(adjust pH to3.6 with triethlamine):Acetonitrile(90∶10),and the detection wavelength was 270 nm.Three concentration levels(20,100,500 μg/kg) of cefquinome in the blank tissues were analysed,the recovery of all samples were exceed 78 %,and the average recovery rates in muscle,liver,kidneys,lung and skin+fat was 81.57 %,82.42 %,81.29 %,83.97 %,78.80 % respectively,the intra-day coefficient of variance was between 1.82 % and 6.25 %,the inter-day coefficient of variance was between 1.11 % and 6.35 %.The limit of detection(LOD) of cefquinome in tissues was 20 μg/kg.The linear ranges of cefquinome sulphate was 20～500 μg/kg.Cefquinome was administered intramuscularly to swines at a dosage of 2 mg/kg for five days.The concentration of medicine in all tissues was detected after the end of the treatment.The result showed that the concentration of cefquinome in lung,skin+fat was declined lower than LOD at the 4 d,and what in others tissues was declined lower than LOD at the 5 d.A 3-day of withdrawal time was recommended." @default.
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- W2384037426 date "2008-01-01" @default.
- W2384037426 modified "2023-09-25" @default.
- W2384037426 title "Detemination cefquinome sulphate in swine tissues and residues after intramuscular injection" @default.
- W2384037426 hasPublicationYear "2008" @default.
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