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- W2384131013 abstract "The method for determination of fumonisins B_1 in corn by High Performance Liquid Chromatography is reported. The sample is extracted with Acetonitrile-0.1?mol/ml NaH_2PO_4(1+1).Filtrate is cleaned up by Sep-pak C_(18) cartridges. Fluorescent fumonisins derivatives are formed by adding OPA and are separated on Shimadzu STR ODS column. Then, they are detected by fluorescent detector and quantified by external standard. Corn samples are fortified with fumonisins B_1 at four levels. Five replicate analyses are performed in each level. The recoveries of the fumonisins B_1 are 82.1%-87.8%.The variation coefficients are 4.7%-7.8%.The detection limit is 0.020?mg/kg." @default.
- W2384131013 created "2016-06-24" @default.
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- W2384131013 date "2004-01-01" @default.
- W2384131013 modified "2023-09-23" @default.
- W2384131013 title "Determination of fumonisins B_1 in corn by solid phase extraction-high performance liquid chromatography" @default.
- W2384131013 hasPublicationYear "2004" @default.
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