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- W2384158703 abstract "A gas chromatography-mass spectrometry method based on internal standard was developed for the rapid determination of musk xylene(MX) in cosmetics.In order to disperse sample matrix into extraction solvent,samples were distributed by use of a vortex mixer,and then extracted on an ultrasonic generator.Therefore,the influences of solvent type,solvent consumption and ultrasonic time on the target extraction efficiency were discussed.Then,the appropriate internal standard was selected.The characteristic ions and its abundance were determined.Chromatographic conditions,such as column flow,injection volume and split ratio,were optimized.Under the optimal conditions,the calibration curve of MX was linear in the range of 0.1 to 4.0 μg/mL with a correlation coefficient of 0.9991,the recoveries for the sample were in the range of 88.44% to 105.94%,with relative standard deviations of 2.05% to 4.67%,the detection limit and quantitative limit of MX were 0.44 mg/kg and 1.45 mg/kg respectively.The results showed that,the method was simple,rapid,sensitive,accurate,and was suitable for the rapid determination of MX in cosmetics." @default.
- W2384158703 created "2016-06-24" @default.
- W2384158703 creator A5042158848 @default.
- W2384158703 date "2013-01-01" @default.
- W2384158703 modified "2023-09-23" @default.
- W2384158703 title "Determination of Musk Xylene in Cosmetics by Using Vortex Mixing Assisted Ultrasonic Extraction and GC/MS Method Based on Internal Standard" @default.
- W2384158703 hasPublicationYear "2013" @default.
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