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- W2384181544 abstract "Objective:To establish a method for the determinantion of 5-hydroxymethylfurfural in Shengqifuzheng injection.Methods:The HPLC separation was performed on a Diamonsil C18 reversed-phase column with the mobile phase of acetonitrile-0.5% acetic acid(3:97),and the determination wavelength was 284 nm.The column temperature was kept at 30 ℃,and the mobile phase flow rate was 1.0 mL·min-1.Results:The calibration curves showed good linear regression(r=0.9999) within 0.94 and 18.8 μg·mL-1.Precisions and repeatabilities of the methods were 0.7% and 2.2%,respectively.Otherwise,only fructose generated 5-hydroxymethylfurfural after high-temperature sterilization.Conclusion:The method was simple,reliable and suitable for the quality control of the products,supplying helpful information to the further study on the safety evaluation of traditional Chinese medicine injection." @default.
- W2384181544 created "2016-06-24" @default.
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- W2384181544 date "2012-01-01" @default.
- W2384181544 modified "2023-09-25" @default.
- W2384181544 title "HPLC determination of 5-hydroxymethylfurfural in Shengqifuzheng injection and preliminary study on the generation approach of 5-hydroxymethylfurfural" @default.
- W2384181544 hasPublicationYear "2012" @default.
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