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- W2384308208 abstract "AIM The aim is to prepare 1 (3 fluoro 2,6 dimethylphenoxy) propanone(Ⅱ-a) and 1 (4 fluoro 2,6 dimethylphenoxy) propanone(Ⅱ-b). METHODS It is prepared %via% 2,6 dimethylphenol by the nitration, reduction, Schiemann reaction, condensation, but different strategies were used while choosing the nitration agents, protective groups, order of the removal of protective groups, and the condition of fluorination when synthesizing two target compounds. RESULTS Two target compounds and intermediate 3 fluoro 2,6 dimethylphenol(Ⅴ-b) were synthesized. The structures of the three compounds were determined by the spectra analysis and elemental analysis. CONCLUSION The two target compounds can be used to synthesize F subsituted analogies of DDPH." @default.
- W2384308208 created "2016-06-24" @default.
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- W2384308208 date "2001-01-01" @default.
- W2384308208 modified "2023-09-23" @default.
- W2384308208 title "Synthesis of 1-(3-and 4-Fluoro-2,6-Dimethylphenoxy) Propanone" @default.
- W2384308208 hasPublicationYear "2001" @default.
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