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- W2384451323 abstract "Di-2-ethylhey α-pinene-maleate,which may be a novel plasticizer,was synthesized by the reaction ofα-terpinene-maleic anhydride adduct(TMA) with 2-ethylhexanol in the presence of toluene-p-sulfonic acid as catalyst.The optimal conditions were obtained by using the orthogonal experimental design,the target product was analyzed and charactertized by means of TLC,IR,MS,1H NMR methors.The optimal conditions were as follows :molar ratio of TMA to 2-ethulhexanol 1∶3.5,reaction temperature 130℃,reaction time 180min,catalyst dosage 1.0%(based on the weight of TMA).The esterification rate amounted to 93% under the opimal conditions,the yield was above 90.3%." @default.
- W2384451323 created "2016-06-24" @default.
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- W2384451323 date "2008-01-01" @default.
- W2384451323 modified "2023-09-22" @default.
- W2384451323 title "Synthesis of Di-2-ethylhexyl α-pinene-maleate" @default.
- W2384451323 hasPublicationYear "2008" @default.
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