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- W2384503964 abstract "Objective To develop a quantitative method for the determination of baicalein in Gujing pill by HPLC. Methods Baicalein was chromatographed on a YWG-NH2 column (4.6 mm ID×250 mm, 5 μm) using a mixture of acetonitrile and water (26∶74 v·v -1 ), which was adjusted to pH 2.6 by phosphoric acid, and monitored at 276 nm with a flow rate of 1.0 ml·min -1 . Results The number of theoretical plates calculated by baicalein peak was 2950. The regression equation was y=796121.5 x +621926.0 (r=0.9999), which was linear over a range from 20.20 μg·ml -1 to 202.0 μg·ml -1 . The average recovery was 100.5% (n=6, RSD 2.1%). Conclusion The method is proved to be sensitive, rapid and accurate." @default.
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- W2384503964 date "2006-01-01" @default.
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- W2384503964 title "Determination of baicalein in Gujing pill by HPLC" @default.
- W2384503964 hasPublicationYear "2006" @default.
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