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- W2384676629 abstract "OBJECTIVE: To prepare Total alkaloids of Sophora alopecuroides( TASa) effervescent suppository and to study its quality standard. METHODS: The suppository was prepared with TASa as principal agent, and the contents of the three alkaloids— Oxymatrine, Matrine and Sophocarpine in the suppository were determined by HPLC with DiamonsiL C18( 150mm× 4. 6mm, 5μ m) used as chromatographic column and mobile phase consisted of acetonitrile-0. 05mol· L-1 K3PO4 buffer solution ( 2‰ triethylamine) =10. 5∶ 89. 5. The UV detection wavelength was 210nm; the column temperature was set at room temperature and the flow rate was 1. 0mL· min-1. RESULTS: The linear ranges for the above 3 alkaloids were 1～ 10, 10～ 60 and 5～ 40μ g· mL-1, respectively. The average recoveries of the three were 76. 63% , 83. 14% and 95. 2% , respectively. The intra-day and inter-day relative standard deviation( RSD) was less than 0. 07% . CONCLUSION: The suppository is simple in preparation, and the established standard can be used as a quality control of this preparation." @default.
- W2384676629 created "2016-06-24" @default.
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- W2384676629 date "2007-01-01" @default.
- W2384676629 modified "2023-09-24" @default.
- W2384676629 title "Preparation and Quality Standard of Total Alkaloids of Sophora Alopecuroides Effervescent Suppository" @default.
- W2384676629 hasPublicationYear "2007" @default.
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