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- W2384711740 abstract "An efficient and safe procedure for the synthesis of arylsulfonylisothiocyanates from readily available aryl sulfonamides and bis(trichloromethyl) carbonate(BTC) was introduced.Aryl sulfonamides and potassium hydroxide were mixed in N,N-dimethylformamide(DMF) and carbon disulfide was added dropwise.The reaction mixture was kept under an atmosphere of nitrogen at 45(°C) for 7.5 h,after which brown potassium aryl sulfonyliminodithiocarbonates were precipitated.Following filtration and vacuum drying,the above salts were suspended in anhydrous dichloroethane,and then a solution of BTC in dichloroethane was added dropwise,and the reaction was continued at 45(°C) for 15 h.The arylsulfonylisothiocynates were obtained in 61%~75% yield." @default.
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- W2384711740 date "2009-01-01" @default.
- W2384711740 modified "2023-09-28" @default.
- W2384711740 title "A Facile Synthesis of Arylsulfonylisothiocynates from Aryl Sulfonamides and Bis(trichloromethyl) Carbonate" @default.
- W2384711740 hasPublicationYear "2009" @default.
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