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- W2384865116 abstract "Objective:For optimization of extracting craft condition of Banxia Baizhu Tianma Decoction with the semi-bionic enzyme extraction,taking gastrodine as comprehensive evaluation one of the index signs,inquiring into the possibility that it uses a HPLC measurement.Methods:Aanreling to the comparison of the prescription taking each Chinese herbal medicine,joining feat enzyme to prepare a processing,Acording to SBE method,adopting to L18(6×36)experiment form,joining feat digest enzyme in the first and third extracting solution,under the feat temperature withdraw a liquid For researching of method of the HPLC measurement.A DiamonsilTM C18 column(5μm,4.6 mm×250 mm) was used.The mobile phase was methyl cyanide-0.05%phosphoric acid(3:97).The detection wavelength was at 220nm.The flow rate was 1mL·min-1,the column temperature was 25℃.Results:The linear rang of gastrodine was 0.87～10.44 μg,r=0.999 6.The average recovery was 101.52%,RSD=1.58%(n= 6).Conclusion:The result is accurate and the reproducibility is good.The method can be used for the determination of gastrodine in Banxia Baizhu Tianma decoction extracted with semi-bionic enzyme extraction" @default.
- W2384865116 created "2016-06-24" @default.
- W2384865116 creator A5009537194 @default.
- W2384865116 date "2008-01-01" @default.
- W2384865116 modified "2023-09-28" @default.
- W2384865116 title "Determination of Gastrodine in Banxia Baizhu Tianma Decoction Extracted by Semi-Bionic Extraction by HPLC" @default.
- W2384865116 hasPublicationYear "2008" @default.
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