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- W2384934252 abstract "1-Bromododecane was synthesized from industrial waste hydrobromic acid and n-dodecyl alcohol using dodecyl dimethyl benzyl ammonium chloride as a phase transfer catalyst. the suitable preparation condition is as follows: the amount of n-dodecyl alcohol is 0.08 mol, the amount of the catalyst is 0.29 mmol, the molar ratio of n-dodecyl alcohol, hydrobromic acid and concentrated sulfuric acid is 1:1.25:1.38, reaction time at refuxing temperature is 3 hours. the yield of 1-bromodecane is 98.8%. the scale-up and repeating experiments are performed which offers the average yield of 98.3%. raw product was analyzed by gc and no by-product was detected. Pure product was characterized by ir and index of refraction." @default.
- W2384934252 created "2016-06-24" @default.
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- W2384934252 date "2009-01-01" @default.
- W2384934252 modified "2023-09-28" @default.
- W2384934252 title "The Improvement of Synthesis of 1-Bromododecane Using Phase Transfer Catalysts Method" @default.
- W2384934252 hasPublicationYear "2009" @default.
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