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- W2385327097 abstract "Taking the sodium methoxide as catalyst,N,N'-1,4-bis(4-methylphenyl) sulfonyl-homopiperzine was synthesized.The effects of material ratio,reaction time,solvent volume,amounts of phase transfer catalyst on the synthesis were studied.So the best technology has been obtained:N,N'-1,4-bis(4-methylphenyl)sulfonylethylenediamine 0.02 mol,the molar ratio of N,N'-1,4-bis(4-methylphenyl)sulfonylethylenediamine to 1,3-dibromopropane is 1 ∶1.25,the reaction time is 13 h,solvent volume of dimethylformamide is 60 mL,benzyl triethyl ammonium bromide is 0.6 g,the best yield of the structure could reach 65.65%." @default.
- W2385327097 created "2016-06-24" @default.
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- W2385327097 date "2008-01-01" @default.
- W2385327097 modified "2023-09-26" @default.
- W2385327097 title "Synthesis of N,N'-1,4-bis(4-methylphenyl) sulfonyl-homopiperzine" @default.
- W2385327097 hasPublicationYear "2008" @default.
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