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- W2385483868 abstract "Objective To establish a high performance liquid chromatography with fluorescence detector for the determination of the benzo(a)pyrene(B(a)P) level in the cooking oil.Methods The difference of B(a)P content in edible oil in Jinan market was investigated by the SHIMADZU shim-pack VP-ODS(250 mm×4.6 mm,5 μm) column.The mobile phase was methanol-water(90∶ 10,V/V),and the flow rate was 1.0 mL/min.The samples were treated by the non-bonded silica solid phase extraction(SPE) column,and then detected at the 285 nm excitation wavelength and 406nm emission wavelength.Results The lowest limit of determination was 0.039 μg/kg(S/N=3).The recovery rate was 85.8%-90.7%,and the intra-day and inter-day relative standard deviations were 2.9%-4.1% and 3.7%-5.3%.Conclusion This method is high sensitive,good selective and quantitative accurate,which is suitable for the B(a)P determination in the cooking oil." @default.
- W2385483868 created "2016-06-24" @default.
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- W2385483868 date "2012-01-01" @default.
- W2385483868 modified "2023-09-26" @default.
- W2385483868 title "Determination of the Benzo(a)pyrene level in cooking oil by solid phase extraction-high performance liquid chromatography" @default.
- W2385483868 hasPublicationYear "2012" @default.
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