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- W2385569946 abstract "Through the reactions of ferrous thiolates with tetrathiomolybdate, we discussed the reaction pathways and possible intermediates during the formation of double-cubane type Mo-Fe-S cluster compounds. We also reported the synthesis, crystal structure, IR and magnetic susceptibi- lity measurements of the title compound 2. The crystal of 2 belongs to triclinic system, M_r=2670.3; P1; a=12.755(4)A, b=13.076(3)A, c=20.576(4) A; α=80.00 (2)°, β=81.39(2)°, γ=61.51(2)°; V=2966.3(14)A~3; Z=1; D_c=1.495 g/cm~2. Final R factor is 0.077 for 4031 observed reflections. The compound was obtained through the reaction of (Et_4N)_2[Fe_4(SPh)_(10)] (1) with (Et_4N)_2MoS_4 in acetonitrile solution. The structure of anion 2 is two cubane clusters bridged by a Fe(SPh)_6 group. The Mo…Mo′ distance of 7.188A is the longest among all double-cubane cluster compounds of known structures." @default.
- W2385569946 created "2016-06-24" @default.
- W2385569946 creator A5047809676 @default.
- W2385569946 date "1986-01-01" @default.
- W2385569946 modified "2023-09-23" @default.
- W2385569946 title "Syntheses and structural studies of molybdenum-iron-sulfur compounds I. The synthesis and crystal structure of (Et_4N)[Mo_2Fe_7S_8(SPh)_(12)]" @default.
- W2385569946 hasPublicationYear "1986" @default.
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