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- W2386115402 abstract "Objective:To study the synthesis of methyl 4-aryl-thiophene-2-carboxylate derivatives.Methods:2-Aryl-Vinamidinium salts were prepared from corresponding arylacetic acid under Vilsmeir-Haack conditions,and then refluxedwith methylthioglycolate under basic conditions(sodium methoxide,methanol) to produce methyl 4-aryl-thiophene-2-car-boxylate derivatives.Results:Ten methyl 4-aryl-thiophene-2-carboxylate derivatives were prepared,five of which were newcompounds.The structures of all products were confirmed by1HNMR and HRMS.Conclusion:Anewsynthetic method ofmethyl 4-aryl-thiophene-2-carboxylate derivatives is developed under moderate reaction condition,with simple operation andhigh yield.A possible reaction mechanism is described." @default.
- W2386115402 created "2016-06-24" @default.
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- W2386115402 date "2006-01-01" @default.
- W2386115402 modified "2023-09-23" @default.
- W2386115402 title "Synthesis of methyl 4-aryl-thiophene-2-carboxylate derivatives" @default.
- W2386115402 hasPublicationYear "2006" @default.
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