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- W2386216337 abstract "Objective To determine the seven main salvianolic acids in Xiangdan injection by the developed HPLC-DAD.Methods The HPLC analysis was performed on a column of Thermo ODS2(4.6 mm×250 mm,5 μm).The mobile phase was acetonitrile and water with 0.05% phosphoric acid.Gradient elution was performed in linear gradient.The flow rate was 1.0 mL/min and detection wavelength was 280 nm.Results The calibration curves of Danshensu,protocatechualdehyde,caffeic acid,rosmarinic acid,lithospermic acid,salvianolic acid B and salvianolic acid A showed good linear regression(r20.999 0) in the investigated concentration ranges.The RSD of precision and the stability in 48 h was less than 1% and 2%,respectively.The average recoveries were between 98% and 103% with RSD2%.The content of the seven components was obviously different in Xiangdan injection obtained from different company.Conclusion This method is simple,reliable,and can be applied for the simultaneous determination of seven salvianolic acids in Xiangdan injection.It can be used for quality control of the medicine." @default.
- W2386216337 created "2016-06-24" @default.
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- W2386216337 date "2012-01-01" @default.
- W2386216337 modified "2023-09-24" @default.
- W2386216337 title "Simultaneous Determination of Seven Salvianolic Acids in Xiangdan Injection by HPLC-DAD" @default.
- W2386216337 hasPublicationYear "2012" @default.
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