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- W2386283538 abstract "25,27-Diisopropoxy-26,28-dihydroxy-calix[4]arene(2) was synthesized by dialkylation of 25,26,27,28-tetrahydroxy-calix[4]arene(1) and 2-iodopropane(i-PrI) using K2CO3 as the catalyst in MeCN.The structure was confirmed by 1H NMR and MS.The optimum reaction conditions were as followed: 1 was 23.8 mmol;n(1) ∶n(K2CO3) ∶n(i-PrI) ∶n(MeCN) was 1.0 ∶1.1 ∶3.3 ∶84.0;ionization time was 1.5 h at 84 ℃;reflux reaction time was 24 h.The yield of 2 was 84.13% with purity of 95%." @default.
- W2386283538 created "2016-06-24" @default.
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- W2386283538 date "2011-01-01" @default.
- W2386283538 modified "2023-09-23" @default.
- W2386283538 title "Synthesis of 25,27-Diisopropoxy-26,28-dihydroxy-calix[4]Arene" @default.
- W2386283538 hasPublicationYear "2011" @default.
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