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- W2386554108 abstract "MnxFe1-xO4 nanoparticles were prepared by coprecipitation with forced mixing. The measurement of magnetic properties indicated that with increasing Mn concentration the specific saturation magnetization of the MnxFe1-xFe2O4 samples decreased at first, and then increased again. The variational trend was also found in estimating particle size. The observation of TEM showed that the size of MnFe2O4 particles was larger than that of Fe3O4 particles. The calculation of Rietveld refinement suggested that the cation distribution of the MnFe2O4 sample was Mn0.3Fe0.7[Mn0.7Fe1.3]O4, and the oxygen parameter and the tetrahedral interstices of the MnFe2O4 sample were larger than those of Fe3O4 sample. The crystallite size and the microstrain of the MnFe2O4 sample were also larger than those of Fe3O4 sample, probably due to its larger ion radius and the metastable cation distribution. The thermal analysis of sample oxidation showed that the temperature for weight gaining from oxidation of the MnFe2O4 sample was higher than that of Fe3O4 sample. The temperature for maximum increase in weight shown in DTG curves was 234.7oC for Fe3O4 and 358.1oC for MnFe2O4, respectively, indicating that the stability against oxidation of MnFe2O4 was improved." @default.
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- W2386554108 date "2004-06-20" @default.
- W2386554108 modified "2023-09-22" @default.
- W2386554108 title "Preparation and Characterization of MnxFe1-xO4 Nanoparticles Coprecipitated with Forced Mixing" @default.
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