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- W2387113068 abstract "Objective Establish a method of quantitative determination of benzoyl peroxide in wheat flour.Method Taking 2.5g samples placed in 25ml colorimetric tube with stopper,before adding 5.0mL methanol,2.5mL KI solution and 5.0mL LHJ solubilizer to sample.After constant volume to 25.0mL and centrifuging,the supernatant was filtered with 0.22 μm filtering membrane and the 10μL filtrate were used for HPLC analysis.The C18 chromatographic column and the mobile phase of mixture of methanol and ammonium acetate(5+95) were used for the separation,flow rate of 1.0mL / min,column temperature 30℃,230nm wavelength UV detector.Results A good linear relationship between values of peak area and mass concentration of benzoyl peroxide was obtained in the range of 0.001 mg / mL ~ 0.100mg / mL,the correlation coefficient was 0.9999,the recovery rate was in the range of 90.6%~102%,precision was in 0.83%~9.50%,the detection limit was 0.00015g/Kg.Conclusions the method was simple and accurate with high recovery rate and good precision.Using the novel LHJ solubilizer in sample preparation,determination results was stable with the very good practical value and promotion prospects." @default.
- W2387113068 created "2016-06-24" @default.
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- W2387113068 date "2012-01-01" @default.
- W2387113068 modified "2023-09-23" @default.
- W2387113068 title "The research on LHJ solubilizer for determination method of benzoyl peroxide in wheat flour" @default.
- W2387113068 hasPublicationYear "2012" @default.
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