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- W2387121626 abstract "Monolauryl citrate was synthesized by regioselective esterification.Reaction of citric acid with paraformaldehyde gave anhydromethylene citric acid(Ⅰ) with a yield of 63%;the reaction of compound(Ⅰ) with acetic anhydride gave the corresponding anhydride(Ⅱ) with a yield of 87%;the esterification of compound(Ⅱ) with lauryl alcohol gave anhydrocitric acid monoester(Ⅲ) with a yield of 76%.Refluxing(Ⅲ) with 1 equivalent of base in aqueous dioxane,the monolauryl citrate was obtained with a yield of 83%.All the compounds were characterized by means of ~(1)H NMR,IR and Elemental Analysis." @default.
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- W2387121626 date "2006-01-01" @default.
- W2387121626 modified "2023-09-22" @default.
- W2387121626 title "Regioselective Synthesis of Monolauryl Citrate" @default.
- W2387121626 hasPublicationYear "2006" @default.
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