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- W2387403009 abstract "1-[5-(4-pentaphenoxy)phenyl-10,15,20-tri(3,4-dichlorophenyl)porphyrin]-5-fluorouracil(A),1-[5-(4-hexaphenoxy)phenyl-10,15,20-tri(3,4-dichlorophenyl)porphyrin]-5-fluorouracil(B)were synthesized from 5-[4-(5-bromo-pentaphenoxy)phenyl]-10,15,20-tri(3,4-dichlorophenyl)porphyrin or 5-[4-(6-bromo-hexaphenoxy)phenyl]-10,15,20-tri(3,4-dichlorophenyl)porphyrin,and characterized by UV-Vis,IR,1HNMR and MS.The synthesis and separation conditions of the target compounds were studied.The yields were higher with DMF as the solvent at 115℃ for 2h.The products were separated via column chromatography with silica gel(200—300)with chloroform,chloroform-ether(V∶V=50∶1)and chloroform-acetone(V∶V=7∶1)as the eluent when the column was 3 cm in diameter and 10 cm in hight." @default.
- W2387403009 created "2016-06-24" @default.
- W2387403009 creator A5030475561 @default.
- W2387403009 date "2010-01-01" @default.
- W2387403009 modified "2023-09-25" @default.
- W2387403009 title "Synthesis and Characterization of Two New Dichloro-Phenyl Porphyrin-5-Fluorouracil Compounds" @default.
- W2387403009 hasPublicationYear "2010" @default.
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