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- W2387850507 abstract "2,2-Dichloro-1,3-benzodioxole(DCBZ) was synthesized,and 2,2-di-(p-nitrophenoxy)-l,3-benzodio -xole(DPBZ) was obtained by using DCBZ reacting with p-nitrophenol. DPBZ was characterized by IR and 1H NMR,and its crystal structure was also determined by X-ray single crystal diffraction,R=0.041 4,Rw=0.104 4. It was observed that the crystal belongs to monoclinic system,space group P2 (1)/c,with a=15.709 3(4) nm,b=8.779 9(2) nm,c= 13.533 6(3) nm,β=102.840 (2)°,V=1 819.96(7) nm3,Z=4. The crystal form supermolecular structure by weak intermolecular hydrogen bonding and π-π stacking. Two p-nitrophenoxys in the DPBZ molecule are distributed in both sides of the plane of the l,3-benzodioxole ring respectively. 6figs.,4tabs.,16refs." @default.
- W2387850507 created "2016-06-24" @default.
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- W2387850507 date "2008-01-01" @default.
- W2387850507 modified "2023-09-23" @default.
- W2387850507 title "Synthesis and Crystal Structure of 2,2-Di-(p-Nitrophenoxy)-l,3-Benzodioxole" @default.
- W2387850507 hasPublicationYear "2008" @default.
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