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- W2387937385 abstract "A method for the determination of hexabromocyclododecane(HBCD) in coatings by GC-MS was proposed.Sample was ultrasonically extracted with dichloromethane-acetone(1+1) mixed solvent,purified by passing through silica gel solid phase extraction column,and quantitatively concentrated with parallel evaporation instrument.DB-5MS capillary column was used for separation,and full-scanning mode and selected ion monitoring mode were adopted in MS determination.Linear relationship between values of peak area and mass concentration of HBCD was kept in the range of 1-50 mg·L-1,with lower limit of determination(10S/N) of 10 mg·kg-1.Tests for recovery were made at the concentration levels of 5,20,50 mg·L-1 of HBCD standard,giving values of recovery and RSD′s(n=8) in the ranges of 82.0%-106% and 2.8%-5.3% respectively." @default.
- W2387937385 created "2016-06-24" @default.
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- W2387937385 date "2012-01-01" @default.
- W2387937385 modified "2023-09-23" @default.
- W2387937385 title "GC-MS Determination of Hexabromocyclododecane in Coatings" @default.
- W2387937385 hasPublicationYear "2012" @default.
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