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- W2388092018 abstract "Four Co(Ⅱ) complexes [Co(btec)0.5(pz)2]n(1),[Co(btec)0.5(pz)3]n(2),[Co(phen)(Hbtc)(H3btc)(H2O)2]·3H2O(3),[Co(Imh)2(anis)2(H2O)](4),(H4btec=1,2,4,5-benzenetetracarboxylic acid,pz=pyrazole,H3btc=1,3,5-benzene-tricarboxylic acid,phen=1,10-phenanthroline,Imh=imidazole,Hanis=p-anisic acid) were synthesized by hydrothermal method.They were characterized by X-ray single crystal diffraction,IR,elemental analysis,UV-Vis-NIR diffuse reflection spectrum and surface photovoltage spectroscopy(SPS).The structural analyses indicate that 1 is a Co(Ⅱ) polymer with 2D structure.The Co(Ⅱ) ion is four-coordinate in 1;the ones in 2～4 are both six-coordinate.2 possesses 1D structure,connected by hydrogen bonds into 2D layer.3 and 4 are molecular complexes,which are networked into 3D and 2D structures by hydrogen bonds,respectively.Four complexes all exhibit obvious surface photovoltage responses within 300～600 nm in SPS,which indicates that they possess certain photo-electric conversion properties.The influences of structure,dimension of complex and coordination micro-environment of center metal ion on the SPS were discussed emphatically.The energy band theory of semiconductor and crystal field theory are combined to analyze and assign SPS response bands.CCDC:883535,1;883536,2;883537,3;883538,4." @default.
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- W2388092018 date "2013-01-01" @default.
- W2388092018 modified "2023-09-25" @default.
- W2388092018 title "Synthesis,Structure and Comparison of Photo-electric Properties of Co(II) Complexes with Benzoic Derivatives Ligand" @default.
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