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- W2388301482 abstract "In this study,a SPE-HPLC method was developed to analyze oxytetracycline (OTC),tetracycline (TC) and chlorotetracycline (CTC) in manure. Manure was first extracted with EDTA-Mcllvaine buffer and then the extraction was enriched by LC-18 SPE column for tetracyclines. The results showed that the recoveries of OTC,TC and CTC in manure were between 51.3%—93.7%. With a mobile phase of 0.01mol·l-1oxalic acid,acetonitrile and methanol(V/V/V=76/16/8,pH=2.5) at wavelength 355 nm,the three tetracyclines were completely separated and the lowest detected limit of OTC,TC and CTC were 0.029mg·kg-1,0.055mg·kg-1and 0.073mg·kg-1,respectively. This method was further applied to the analysis of manures collected from animal farms in Anhui province. OTC,TC and CTC were detected in all hen manure,pig manure and in some of the cow manure." @default.
- W2388301482 created "2016-06-24" @default.
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- W2388301482 date "2010-01-01" @default.
- W2388301482 modified "2023-10-03" @default.
- W2388301482 title "DETERMINATION OF OXYTETRACYCLINE,TETRACYCLINE AND CHLORTETRACYCLINE IN MANURE BY SPE-HPLC METHOD" @default.
- W2388301482 hasPublicationYear "2010" @default.
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