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- W2388656566 abstract "Two Mo/S complexes:K_6[Mo_2O_2S_2(C_2O_4)_2(ClPO_3)_2]·H_2O(1)andK_6[Mo_2O_3S(C_2O_4)_2(ClPO_3)_2]·3H_2O(2)containing oxalate ligand were prepared by the reaction of(NH_4)_2MoS_4 and potassiu oxalate with adding a small amount of H_3PO_4 to adjust the value of pH in system of methanol and water under an atmosphere of pure nitrogen at ambient temperature and charcterized by the means of elemental analysis,IR,UV-vis.The analysis results reveal that crystal of the complex 1 is Orthorhombic,space group pbcn,a=4.6370(2)nm,b=0.7549(2)nm,c=1.3888(4)nm,V=4.861(2)nm~3,Z=8,Mr=945.49,Dc=2.58g/cm~3,μ=2.625cm~(-1),R=0.063,wR=0.075.In addition,The their spectral properties were also discussed." @default.
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- W2388656566 date "2006-01-01" @default.
- W2388656566 modified "2023-09-27" @default.
- W2388656566 title "Synthesis,spectra and crystal structure of a series of Mo/S(O) complexes containing oxalate ligand" @default.
- W2388656566 hasPublicationYear "2006" @default.
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