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- W2388874348 abstract "Microwave irradiation was used to the Knoevenagel-Doebner synthesis of cinamic acid from benzaldehyde and malonic acid using pyridine as a catalyst.The influence of the mol ratio of benzaldehyde and malonic acid,the microwave power,the time of the reaction and the dosage of the catalyst on the yield of cinamic acid was investigated.The optimum reaction con- dition was determined through orthogonal design as follows:the mol ratio of benzaldehyde and malonic acid was 1:2.5,the dosage of pyridine was 2.5mL,the microwave Power was 60% and the time of the reaction was 18 min when 1.5mL of benzaldehyde was used.The refined yield reached 46.7%.In the summary,synthesis of cinamic acid under microwave irradiation in the absence of solvent is high yield and convenient operation and has extensive utilization." @default.
- W2388874348 created "2016-06-24" @default.
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- W2388874348 date "2005-01-01" @default.
- W2388874348 modified "2023-09-25" @default.
- W2388874348 title "Synthesis of Cinamic Acid under Microwave Irradiation in the Absence of Solvent" @default.
- W2388874348 hasPublicationYear "2005" @default.
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