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- W2389030699 abstract "The curing kinetics during vulcanization of polysulfide sealant was investigated using both Differential Scanning Calorimetric method and viscometric method.The heat of curing reaction during vulcanization was measured over the temperature range of 20-40℃ by the non-isothermal and isothermal DSC,the degree of cure and the rate of cure were determined using the data generated by DSC.The activation energy,reaction rate constant and reaction order with on the temperature dependence were obtained by nonlinear fitting method,and the curing kinetics of polysulfide sealant was described subsequently by a modified Kamal kinetic model.Predictions of the rate of cure and the degree of cure by the modified Kamal model agreed with the experimental data.The results indicate the autocatalytic effect in preliminary stage of curing of polysulfide sealant(up to the degree of cureα0.4),and the diffusion-control effect in later stage.The viscosity was measured as a function of time over the temperature range of 20-30℃,an empirical model correlated the viscosity with temperature and the degree of cure was obtained,predictions of the viscosity change by the empirical model agreed with the experimental data up to the degree of cureα0.4." @default.
- W2389030699 created "2016-06-24" @default.
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- W2389030699 date "2015-01-01" @default.
- W2389030699 modified "2023-09-27" @default.
- W2389030699 title "Curing Kinetics of Vulcanization of Polysulfide Sealant" @default.
- W2389030699 hasPublicationYear "2015" @default.
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