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- W2389034043 abstract "AIM To determine six different speciations of arsenic and soluble arsenic in Realgar and five kinds of Chinese patent medicines by HPLC-ICP-MS.METHODS The soluble arsenic was respectively extracted by different solvents and methods: simulated intestinal fluid at the adsorptional condition of 37 ℃,0.16% hydrochloric acid solution with ultrasonic treatment,methanol-water(1∶ 1) with ultrasonic treatment and methanol-water(1∶ 1) with accelerated solvent extraction(ASE).The total quantities of the solvable arsenic was detected by ICP-MS.The speciation of the soluble arsenic was detected by HPLC-ICP-MS.RESULTS The acid-soluble arsenic in different samples only were 0.12 to 2.70 percentage of their total arsenic.Only the speciation of As3+ and As5+ were detected in the soluble arsenic with different solvents.The total quantity of As3+ and As5+ in the acid solvable arsenic were equal to the amount of the acid solvable arsenic in some samples,but not in all samples.CONCLUSION The contents of acid-soluble arsenic were far less than the total arsenic in Realgar and its Chinese patent medicines.Other components in the Chinese patent medicines with Realgar may inhibit the poisonous speciations of the soluble arsenic." @default.
- W2389034043 created "2016-06-24" @default.
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- W2389034043 date "2012-01-01" @default.
- W2389034043 modified "2023-09-23" @default.
- W2389034043 title "Speciations of soluble arsenic in five Chinese patent medicines by HPLC-ICP-MS" @default.
- W2389034043 hasPublicationYear "2012" @default.
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