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- W2389401044 abstract "Mineral sample was dissolved in HNO3,HF and H2SO4,and gallium trichloride was extracted with n-butyl acetate in 6 mol/L HCl.Then,gallium trichloride was back extracted with water in n-butyl acetate,so that trace amounts of gallium could be enriched and separated from other elements which might interfere with the detection.By inductively coupled plasma atomic emission spectrometry,the content of gallium in the sample was determined at the wavelength of 294.364{114} nm.The mechanism of extraction,technology of extraction and seperation,and elimination of disturbing elements were discussed.The instrument parameters were optimized.There was a good linear relationship between emission intensity of gallium and mass concentration of Ga in the range of 0-3 μg/mL.The correlation coefficient of calibration curve was 0.999 9,and the detection limit of this method was 0.052 μg/mL.The content of gallium in certified reference materials was determined by this method and the results were consistent with the certified values with a relative standard deviation(n=6)between 0.85%-1.9%." @default.
- W2389401044 created "2016-06-24" @default.
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- W2389401044 date "2010-01-01" @default.
- W2389401044 modified "2023-09-26" @default.
- W2389401044 title "Determination of gallium in ore by inductively coupled plasma atomic emission spectrometry after preconcentration through extraction" @default.
- W2389401044 hasPublicationYear "2010" @default.
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