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- W2390120733 abstract "OBJECTIVE To establish a ion pair RP HPLC method for the determination of gemcitabine in human plasma METHODS Samples were prepared by protein precipitation. The column was Waters Symmetry C 18 (4 6 mm×250 mm,5 μm) and the temperature was set at 25℃ The mobile phase was 0 52% phosphate buffer(pH 2 66) acetonitrile(85∶15) containing 0 202% sodium 1 heptanesulfonate and the flow rate was 1 0 mL·min -1 The detection wavelength was at 273 nm RESULTS The range of calibration curve was 0 1～100 μg·mL -1 ( r =0 999 9) The recovery of low, medium and high concentration were within 97 39%～103 11% The RSD of intra run and inter run did not exceed 1 94% and 7 34% respectively CONCLUSION The method is rapid, sensitive and efficient" @default.
- W2390120733 created "2016-06-24" @default.
- W2390120733 creator A5091477288 @default.
- W2390120733 date "2005-01-01" @default.
- W2390120733 modified "2023-09-22" @default.
- W2390120733 title "Determination of gemcitabine in human plasma by ion-pair RP-HPLC" @default.
- W2390120733 hasPublicationYear "2005" @default.
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