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- W2390220393 abstract "p-Bromophenyl-methoxy triethylene glycol(3) was prepared by esterification of p-tolylsulfonyl chloride with methoxy triethylene glycol,then condensation with p-bromophenol.Novel 5-bromo-2-[p-(methyl triethylene glycol group)phenyl]pyrimidine(1a) in yield of 73% was selectively synthesized using Pd(PPh_3)_4 as a catalyst in toluene under Ar gas by Suzuki-coupling of 5-bromo-2-iodopyrimidine(5) and p-(methyl triethylene glycol group)phenyl-boric acid(4) which was obtained by substitution reaction of 3 with methyl borate,then acidolysis.Novel 5-bromo-2-dodecylpyrimidine(1b) in yield of 82% was selectively synthesized by Suzuki-coupling in one-pot from 1-dodecylene and 5 using Pd(dppf)Cl_2 as a catalyst in THF.The structures of 1a and 1b were characterized by 1H NMR,13C NMR and MS." @default.
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- W2390220393 date "2011-01-01" @default.
- W2390220393 modified "2023-09-23" @default.
- W2390220393 title "Selective Synthesis of Novel 5-Bromopyrimidine Derivatives" @default.
- W2390220393 hasPublicationYear "2011" @default.
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