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W2390420164 abstract "Under N2 atmosphere,five Nsubstituted4aminophthalimides(Ⅰ) and triphosgene reacted in ethyl acetate for 4 h at -10-0 ℃ and 8 h at room temperature to give corresponding N,N′bis(2substituted1,3dioxo2,3dihydro1Hisoindol5yl)urea(Ⅱ) in 70%-90% yield and (2substituted1,3dioxo2,3dihydro1Нisoindol5yl)carbamic acid ethyl ester(Ⅲ) in 10%-27% yield.Structures of (Ⅲ) were confirmed by1HNMR,IR,elementary analysis and FABMS." @default.
W2390420164 created "2016-06-24" @default.
W2390420164 creator A5081383733 @default.
W2390420164 date "2003-01-01" @default.
W2390420164 modified "2023-09-25" @default.
W2390420164 title "The Synthesis of (2-Substituted-1,3-dioxo-2,3-dihydro- 1Н-isoindol-5-yl)carbamic Acid Ethyl Ester by Triphosgene" @default.
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