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- W2390799905 abstract "The method of the synthesized of dibutyl phosphate from phosphorous acid and butanol was studied.Effects of reaction conditions,such as the ratio of raw materials,reaction temperature,reaction time,catalyst,and reaction time were investigated.The methods of analysis were defined.The composition of product was analyzed by titration method.The result showed: the best temperature was 125-135℃,the mole ratio of n-butanol / phosphorous acid was 3.6,the best reaction time without catalyst was 3h,the yield of dibutyl phosphate was 68%.The product can be separated by the n-butanol/benzene 10:1 in TLC." @default.
- W2390799905 created "2016-06-24" @default.
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- W2390799905 date "2011-01-01" @default.
- W2390799905 modified "2023-09-27" @default.
- W2390799905 title "Study on Synthesis Technology of Dibutyl Phosphate" @default.
- W2390799905 hasPublicationYear "2011" @default.
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