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- W2390821000 abstract "The coordination compound of {[Cd(NTO)2(CHZ)]·2H2O}n was prepared by the reaction of cadmium salt of 3 nitro 1,2,4 triazol 5 one (NTO) with carbohydrazide (CHZ) in solution. The crystal structure of {[Cd(NTO)2(CHZ)]was determined by X ray diffraction analysis. Thermal decomposition mechanismof the compound was studied using TG DTG, DSC and IR techniques. The crystalsbelong to orthorhombic with space group Pbca. The unit cell parameters are as follows:a=0.8623(1)nm, b=1.8259(4)nm, c=1.9997(3)nm, Z=8, R1=0.0517, wR2=0.0655. The coordination number of the cadmium cation is six and the Cd2+ ion shows a distorted octahedral geometry. The NTO serves as a bridging bidentate ligand, coordinated to two cadmium cations with its carbonyl oxygen atom and the nitrogen atom of 4 position. The CHZ serves as a tri dentate ligand, coordinated to acadmium cation with its carbonyl oxygen atom and one of the two nitrogen atoms.At the same time, it is coordinated to the second cadmium cation using other end nitrogen atom. The results demonstrate that the three dimensional infinite super molecular network is constructed." @default.
- W2390821000 created "2016-06-24" @default.
- W2390821000 creator A5037709424 @default.
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- W2390821000 date "2002-01-01" @default.
- W2390821000 modified "2023-09-28" @default.
- W2390821000 title "Preparation, Crystal Structure and Thermal Decomposition Mechanisms of {[Cd(NTO)_2(CHZ)]·2H_2O}_n" @default.
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