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- W2390857489 abstract "A method was established for the simultaneous determination of seven sulfonylurea hypoglycemic agents( e. g. glipizide, tolbutamide, tolazamide, gliclazide, glibenclamide, glimepiride and glurenor) in health care products by solid phase extraction / high performance liquid chromatography( SPE / HPLC). Various samples were extracted with methanol by ultrasound,the extract was cleaned up and concentrated on an LC-C18SPE column. The chromatographic separation was performed on an Agilent Zorbax SB-C18column( 250 mm × 4. 6 mm,5 μm) using acetonitrile( A)-0. 02% phosphoric acid solution( B) as mobile phase by gradient elution at a flow rate of 1. 0 mL /min,a column temperature of 30 ℃ and an ultraviolet( UV) detection wavelength of 228 nm. The seven sulfonylurea hypoglycemic agents showed good linear relationships in the range of 0. 2-20 μg /mL with correlation coefficients larger than 0. 999 9. The limits of detection( S / N≥3) were 0. 1 mg /kg for seven target compounds. The spiked recoveries of seven target compounds in five different health care products ranged from 81% to 115% with relative standard deviations less than 9%." @default.
- W2390857489 created "2016-06-24" @default.
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- W2390857489 date "2013-01-01" @default.
- W2390857489 modified "2023-09-26" @default.
- W2390857489 title "Simultaneous Determination of Seven Sulfonylurea Hypoglycemic Agents in Health Care Products by Solid Phase Extraction / High Performance Liquid Chromatography" @default.
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