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- W2391051489 abstract "A high-performance liquid chromatography-tandem mass spectrometric method was established for the determination of residue of hydrocortisone(HYD) in fishery products. HYD was extracted from homogenized samples with ethyl acetate and n-hexane; the filtrate was purified by solid-phase extraction with Oasis HLB cartridge. Analyte identification was performed by electrospray ionization(ESI) in negative mode using MRM and the quantification was performed using external standard method. The limit of quantification was 2.0 ng/g, and the linear range was 2~200 ng/mL. At spiked level of 2.0～10.0 ng/g, the average recoveries of HC were 99.3%~106.0%, RSD were 2.62%~7.71%. The method was sensitive, reliable, selective and specific for the determination of hydrocortisone residue." @default.
- W2391051489 created "2016-06-24" @default.
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- W2391051489 date "2009-01-01" @default.
- W2391051489 modified "2023-09-23" @default.
- W2391051489 title "High-performance liquid chromatography-tandem mass spectrometry for determination of residue of hydrocortisone in fishery products" @default.
- W2391051489 hasPublicationYear "2009" @default.
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