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- W2391377900 abstract "Objective:To establish a method for the determination of the residual solvents for methanol,ethanol and ethyl ether in Risedronate.Methods:The determination was performed by GC with a glass column which was packed by SE-30(30m×0.530mm,1.00μm)and the columm temperature was 40℃,and the detector was FID with maintaining the temperature at 300℃,and the vector was nitrogen,and the flow rate was 40ml/min.Results:Under the experiment condition,the methanol,ethanol and ethyl ether were separated thoroughly and each solvent had a good linear relationship within a certain range(r=0.998 8~0.999 0);the average recovery was 92.8%~97.7%,and the RSD was 1.2%~3.9%;The detection limits of methanol,ethanol and ethyl ether were 1.294,1.630,3.164μg/ml respectively.Conclusion:The method is accurate and sensitive.It can be used for the determination of the residual solvents in Risedronate." @default.
- W2391377900 created "2016-06-24" @default.
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- W2391377900 date "2011-01-01" @default.
- W2391377900 modified "2023-09-24" @default.
- W2391377900 title "Determination of Residual Solvents in Risedronate by GC" @default.
- W2391377900 hasPublicationYear "2011" @default.
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