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- W2391465216 abstract "OBJECTIVE To establish a method for the determination of impurity oxalic acid in Oxaliplatin by HPLC.METHODS C18 column(AQ 5μm 4.6mmI.D.×250mm) was used.phosphate buffer(40% tetrabutylammonium hydroxide was proper in the water and adjusted to pH 6.0 with phosphoric acid):acetonitrile(80∶ 20) was used as a mobile phase;the flow rate was 2.0mL·min-1;the column temperature was set at 40℃ and the detection wavelength of UV detector was 205 nm.RESULTS The linear range of impurity A was 0.36-3.6μg·mL-1(r=0.9991);the limits of the quantitation and qualification of impurity A were 1.45μg·mL-1 and 0.36μg·mL-1.CONCLUSION The method is proved to be simple and accurate.It is suitable for determination of impurity B in Oxaliplatin." @default.
- W2391465216 created "2016-06-24" @default.
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- W2391465216 date "2013-01-01" @default.
- W2391465216 modified "2023-09-23" @default.
- W2391465216 title "Exploration and determination of impurity Oxalic acid in Oxaliplatin" @default.
- W2391465216 hasPublicationYear "2013" @default.
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