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- W2391570787 abstract "Poly(e-caprolactone)s (PCLs) with different molecular weight were cross-linked by γ-radiation.The radiation crosslinking feature was examined by Soxhlet extractor with toluene and analyzed by using the Charlesby-Pinner equation.The crosslinking degree is related to molecular weight and radiation dose,and the relation between the sol fraction and the radiation dose follows the Charlesby-Pinner equation.Radiation may cause a drop of tensile strength and elongation for all the samples d.The DSC diagrams demonstrated that radiation caused an increase of crystallinity and a decrease of melting temperature of PCL crystals.The DMA analysis indicated that radiation crosslinking raised heat deformation temperature of PCL and caused a rubbery state after the melting of PCL crystals.The shape memory results indicated that only those specimens that had a sufficiently high cross-linking degree (gel content is higher than about 15%) were able to show the typical shape memory effect,a large recoverable strain and a high final recovery rate.The response temperature of the recovery effect (about 55℃) was related to the melting point of the samples.The PCL shape memory polymer was characterized by its low recovery temperature and large recovery deformation." @default.
- W2391570787 created "2016-06-24" @default.
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- W2391570787 date "2003-01-01" @default.
- W2391570787 modified "2023-09-25" @default.
- W2391570787 title "RADIATION EFFECTS ON STRUCTURE AND PROPERTIES OF POLY(ε-CAPROLACTONE)" @default.
- W2391570787 hasPublicationYear "2003" @default.
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