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- W2392040315 abstract "Continuous Silicalite-1 zeolite membranes on macroporous α-Al_2O_3 supports were prepared through hydrothermal treatment by using coating technique with nanoseeds from clear solution.The prepared seeds,substrate,seeded substrate and Silicalite-1 membranes were characterized by SEM and XRD.The influence of synthesis temperature(130 ℃ and 160 ℃) on the structure of Silicalite-1 membranes was also investigated.It has been shown that pure and uniform Silicalite-1 seeds of about 100 nm serve as a good seed during the growth synthesis,and that a seed layer is formed on the substrate surface by seeding with the nanosized Silicalite-1 seeds,though the substrate possesses uneven pore sizes and coarse surfaces.A dense and free-defect Silicalite-1 zeolite membrane of 4~5 μm thickness has been obtained on the seeded support by the following hydrothermal treatment from clear solution.The seed layer greatly improves the substrate surface and favors the formation of Silicalite-1 membranes.The substrate,seed layer and zeolite film are firmly combined together.The increase of synthesis temperature may alter the orientation of zeolite crystal growth.The method has proven to be effective and allows for the preparation of other type of zeolite membranes on this type of supports." @default.
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- W2392040315 date "2006-01-01" @default.
- W2392040315 modified "2023-09-25" @default.
- W2392040315 title "Synthesis and structural analysis of Silicalite-1 membranes by coating technique with nanosized seed" @default.
- W2392040315 hasPublicationYear "2006" @default.
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