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- W2392214458 abstract "With dicyclohexylcarbodiimide(DCC) as reagent and 4-dimethylaminopyridine(DMAP) as catalyst,the compound 4a(p-phenylene di-13-cis-retinoates) with novel structures and potential bioactivity was synthesized from 13-cis-retinoic acid,and a yield of 87.6% was obtained.The optimized conditions are :2.02 portions of 13-cis-retinoic acid and one portion of quinol were added into a flask,stirring 4 h after DCC was added at a rate of 0.5 drop per second.Other five diesters were synthesized from all-trans-retinoic acid and 13cis-retinoic acid under similar conditions.Then 4a was modified to obtain the anologue of metabolization in the body,and a yield of 75.3% was obtained.Their structures were characterized by()~1H,~(13)C NMR and MS." @default.
- W2392214458 created "2016-06-24" @default.
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- W2392214458 date "2006-01-01" @default.
- W2392214458 modified "2023-09-27" @default.
- W2392214458 title "Synthesis and Characterization of all-trans-Retinoic Acid and 13-cis-Retinoic Acid Diester Derivatives" @default.
- W2392214458 hasPublicationYear "2006" @default.
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