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- W2392567181 abstract "Objective:To establish a determination method of palonosetron level in plasma.Methods:LC conditions were as follows:Hypersil GOLD(150 mm × 4.6 mm,5 μm)was used with the mobile phase consisting of acetateamine buffer(0.1% formic acid)-method(50∶50).Equipped with an atmospheric pressure chemical ionization(APCI)source was used as detector.The plasma samples added with internal standard were extracted with Acetic Ether,then concentrated and determined by LC-MS /MS.Results:The linear range of palonosetron was 0.04～20.00 ng /ml.The lower limit of quantification(LLOQ)was 0.04 ng /ml.The recoveries of palonosetron at low,middle and high concentration and the intra-day and inter-day RSDs all met the standards.Conclusion:The established method is sensitive,specific,reproducible and suitable for studies of pharmacokinetics and detection of plasma drug concentration of palonosetron." @default.
- W2392567181 created "2016-06-24" @default.
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- W2392567181 date "2011-01-01" @default.
- W2392567181 modified "2023-09-25" @default.
- W2392567181 title "Determination of palonosetron in plasma by HPLC-APCI-MS" @default.
- W2392567181 hasPublicationYear "2011" @default.
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