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- W2392869692 abstract "OBJECTIVE To develop a HPLC method for the determination of related substances in Doxepin Hydrochloride.METHODS The column was C18 with a mobile phase of 0.2mol·L-1 sodium dihydrogen phosphate contained 0.1% triethylamine(pH=2.5)-methanol by gradient elution.The flow rate was 1mL·min-1,the detection wavelength was at 254nm.The injection volume was 20μL and column temperature was 50℃.RESULTS The related substances were completely separated from Doxepin Hydrochloride and intermediates and impurities that had smaller polarity could be detected by using this method.The detection limits of Doxepin Hydrochloride was 0.2μg·mL-1.CONCLUSION The method was rapid and simple,accurate and sensitive.It can be used to test the related substances of the product." @default.
- W2392869692 created "2016-06-24" @default.
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- W2392869692 date "2011-01-01" @default.
- W2392869692 modified "2023-09-26" @default.
- W2392869692 title "Determination of related substances in Doxepin Hydrochloride by HPLC" @default.
- W2392869692 hasPublicationYear "2011" @default.
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